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And (2) carrying out suction filtration, adding 120ml of ethyl acetate into the filter cake, carrying out oil bath reflux for 1h at the temperature of 90 ℃, closing and heating, naturally cooling to room temperature, carrying out suction filtration, adding 140ml of triethylamine aqueous solution containing 2.4ml into the filter cake, stirring for 2h at the room temperature, carrying out suction filtration, adding tetrahydrofuran into the filter cake: 140ml of purified water is added in a ratio of 1:1, and after refluxing at 80 ℃ until the mixture is completely clear, heating and stirring are stopped, and the mixture is crystallized at room temperature